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. 2021 Sep 9;11(48):30156–30171. doi: 10.1039/d1ra04092h

Melting temperature, the heat of fusion, and the degree of crystallinity of PVA powder, GLE powder, and PVA/GLE hydrogela.

Sample T m (°C) Δ m (J g−1) during PVA melting Degree of crystallinity (%)
PVA 222; 253; 439 44.80 ± 1.28t 32.31 ± 0.08t
GLE 192; 325
PGL0 221; 250; 423 10.81 ± 0.85u 7.80 ± 0.03u
PGL1 218; 414 7.41 ± 0.56v 5.34 ± 0.02v
PGL2 214; 340 5.17 ± 0.64w 3.73 ± 0.04w
PGL3 213; 337 4.36 ± 0.38w 3.14 ± 0.03x
PGL4 211; 336 3.52 ± 0.35w,x 2.53 ± 0.05y
PGL5 209; 334 1.78 ± 0.42x 1.28 ± 0.03z
a

The value of heat of fusion, and degree of crystallinity was expressed as mean ± SD of 3 samples (n = 3). The use of superscripts on each column represent the statistical significant differences between groups. The groups with the same superscripts within each column indicate that the values are considered not significantly different (p > 0.05).