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. 2021 Sep 21;11(50):31159–31173. doi: 10.1039/d0ra10894d

Summary of the different methods used to synthesize niobium selenide materials, specifically Nb2Se9 and NbSe2.

Material Synthetic method Properties Reference
NbSe2 (a) mechanical exfoliation (a) 1 μm to 30 μm with a thickness less than 2 μm 7
(b) liquid exfoliation (b) micro/nanoplatets range from 0.1 μm to 25 μm with a thickness less than 1 μm 8
(c) RF magnetron sputtering (c) 1.5 μm in thickness 9
(d) chemical vapor transport (d) 10 mm flakes 10
Nb2Se9 (a) flux method (a) 117 nm to 547 nm nanowires 11
(b) mechanical exfoliation (b) 30 nm to 160 nm flakes 12
(c) sintering in evacuated quartz tube (c) single crystals 13