Effects of caprinoyl chloride and NEt3 equivalents on yields of 2d and 3da.
| Entry | Caprinoyl chloride (equiv.) | NEt3 (equiv.) | Yield (%) | |
|---|---|---|---|---|
| 2d | 3d | |||
| 1 | 1.2 | 1.2 | 75 | ND |
| 2 | 2.2 | 1.2 | 74 | ND |
| 3 | 2.2 | 2.2 | 19 | 52 |
| 4 | 5 | 5 | ND | 91 |
a
ND = not detected.
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