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. 2021 Oct 22;11(54):34338–34342. doi: 10.1039/d1ra05932g

Isolated yields of trioxolane adducts obtained under either conventional reaction condition A (in CCl4, 0 °C) or low temperature condition B (in hexane, −78 °C).

graphic file with name d1ra05932g-u1.jpg
Product (3a–f) A: CCl4, 0 °C B: hexane, −78 °C
3a graphic file with name d1ra05932g-u2.jpg 48–91% 91%
3b graphic file with name d1ra05932g-u3.jpg 28%a 50%
3c graphic file with name d1ra05932g-u4.jpg 23% 77%
3d graphic file with name d1ra05932g-u5.jpg 5% 85%
3e graphic file with name d1ra05932g-u6.jpg 18% 94%
3f graphic file with name d1ra05932g-u7.jpg 0% 81%
a

Calculated yield based on 1H NMR.