Boehmite based nano-catalyzed for synthesis of 5-substituted-1H-tetrazole containing scaffolds via [3+2] cycloaddition reaction.
Entry | Boehmite@nano-structures | Catalyst loading (mg or mol%) | Temperature (°C) | Solvent | Time (h) | Yield (%) | Ref. |
---|---|---|---|---|---|---|---|
1 | Pd-SMTU@boehmite | 0.30 mol% | 120 | PEG-400 | 2.5 | 95 | 37 |
2 | Boehmite@SiO2@Tris-Cu(i) | 0.20 mol% | 120 | PEG-400 | 2 | 97 | 38 |
3 | Boehmite Nps@Cur-Ni | 40 mg | 120 | PEG-400 | 1.25 | 97 | 39 |
4 | Ni-SMTU@boehmite | 25 mg | 120 | PEG-400 | 1.33 | 94 | 32 |
5 | Pd-isatin@boehmite | 35 mg | 120 | PEG-400 | 7 | 96 | 36 |
6 | Pd-Arg@boehmite | 25 mg | 120 | PEG-400 | 7 | 97 | 40 |