Reaction time and yield of both conventional, ultrasonic and microwave assisted synthesis of the synthesized compounds.
Comp. | Time (min) | Yield | ||||
---|---|---|---|---|---|---|
Ca | USa | MWa | Ca | USa | MWa | |
4a | 180 + 240 | 10 + 15 | 2 + 2 | 55 | 77 | 88 |
4b | 180 + 240 | 10 + 15 | 2 + 2 | 54 | 79 | 90 |
4c | 180 + 240 | 10 + 15 | 2 + 2 | 56 | 77 | 88 |
4d | 180 + 240 | 10 + 15 | 2 + 2 | 54 | 66 | 90 |
4e | 180 + 240 | 10 + 15 | 2 + 2 | 57 | 60 | 92 |
4f | 180 + 240 | 10 + 15 | 2 + 2 | 49 | 62 | 93 |
4g | 180 + 240 | 10 + 15 | 2 + 2 | 58 | 67 | 92 |
4h | 180 + 240 | 10 + 15 | 2 + 2 | 55 | 78 | 90 |
4i | 180 + 240 | 10 + 15 | 2 + 2 | 53 | 62 | 95 |
4j | 180 + 240 | 10 + 15 | 2 + 2 | 56 | 78 | 91 |
4k | 180 + 240 | 10 + 15 | 2 + 2 | 50 | 77 | 88 |
5a | 180 + 240 | 10 + 15 | 2 + 2 | 57 | 68 | 92 |
5b | 180 + 240 | 10 + 15 | 2 + 2 | 60 | 77 | 93 |
8a | 180 + 240 | 10 + 15 | 2 + 2 | 62 | 79 | 94 |
8b | 180 + 240 | 10 + 15 | 2 + 2 | 56 | 71 | 93 |
8c | 180 + 240 | 10 + 15 | 2 + 2 | 54 | 62 | 95 |
8d | 180 + 240 | 10 + 15 | 2 + 2 | 55 | 78 | 91 |
8e | 180 + 240 | 10 + 15 | 2 + 2 | 51 | 77 | 88 |
8f | 180 + 240 | 10 + 15 | 2 + 2 | 52 | 79 | 90 |
8g | 180 + 240 | 10 + 15 | 2 + 2 | 56 | 79 | 90 |
8h | 180 + 240 | 10 + 15 | 2 + 2 | 50 | 70 | 92 |
8i | 180 + 240 | 10 + 15 | 2 + 2 | 53 | 73 | 93 |
8j | 180 + 240 | 10 + 15 | 2 + 2 | 55 | 67 | 90 |
8k | 180 + 240 | 10 + 15 | 2 + 2 | 45 | 69 | 95 |
8l | 180 + 240 | 10 + 15 | 2 + 2 | 54 | 78 | 91 |
9a | 180 + 240 | 10 + 15 | 2 + 2 | 60 | 60 | 90 |
9b | 180 + 240 | 10 + 15 | 2 + 2 | 61 | 77 | 94 |
C: conventional, US: ultrasonic, MW: microwave.