Effects of the AgF₂ : S₄N₄ molar ratio on the yield of NSF₃^a.

Entry	Molar rate (AgF2/S4N4)	Reaction time/h	Temperature/°C	Yieldb/(%)
1	8 : 1	2	78	21.32
2	10 : 1	2	78	32.32
3	12 : 1	2	78	44.79
4	14 : 1	2	78	53.44
5	16 : 1	2	78	57.38
6	18 : 1	2	78	58.27

^aReaction conditions: S₄N₄ (3 mmol), CCl₄ (waterless, 30 mL), and AgF₂ were added in the specified proportions under stirring.

^bIsolated yield.