13C NMR dataa (δ in ppm, 150 MHz) of 1–10, 13, and 14.
| No. | 1b | 2c | 3b | 4c | 5c | 6c | 7c | 8b | 9b | 10b | 13b | 14c |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 1 | 40.6 | 40.2 | 39.9 | 39.5 | 39.5 | 39.6 | 39.7 | 40.3 | 40.2 | 40.2 | 40.1 | 41.4 |
| 2 | 27.4 | 27.8 | 27.8 | 27.7 | 27.7 | 28.1 | 28.1 | 27.4 | 28.1 | 27.4 | 27.9 | 28.3 |
| 3 | 76.2 | 75.3 | 76.0 | 75.4 | 75.4 | 75.1 | 75.2 | 76.1 | 76.1 | 76.1 | 76.1 | 75.3 |
| 4 | 54.8 | 54.5 | 55.4 | 54.3 | 54.3 | 54.8 | 54.9 | 55.0 | 55.0 | 54.9 | 55.0 | 55.2 |
| 5 | 52.5 | 51.7 | 52.7 | 51.9 | 51.9 | 51.8 | 51.9 | 51.8 | 51.9 | 52.1 | 51.9 | 51.9 |
| 6 | 22.4 | 22.0 | 22.0 | 21.7 | 21.7 | 21.7 | 21.8 | 21.4 | 21.4 | 21.5 | 21.4 | 21.4 |
| 7 | 41.6 | 41.0 | 35.5 | 37.3 | 37.3 | 33.9 | 34.1 | 33.6 | 33.7 | 34.9 | 33.6 | 34.4 |
| 8 | 40.3 | 39.3 | 42.6 | 39.3 | 38.4 | 43.4 | 40.7 | 46.8 | 46.5 | 44.2 | 47.3 | 43.9 |
| 9 | 58.7 | 58.1 | 57.8 | 60.5 | 60.4 | 48.4 | 48.5 | 61.3 | 61.2 | 60.7 | 62.0 | 58.2 |
| 10 | 38.9 | 38.3 | 41.7 | 37.9 | 37.9 | 38.0 | 38.1 | 37.6 | 37.8 | 37.7 | 37.9 | 39.6 |
| 11 | 75.3 | 74.9 | 78.4 | 73.3 | 73.3 | 77.1 | 77.1 | 196.2 | 196.1 | 196.2 | 196.0 | 73.2 |
| 12 | 214.1 | 213.0 | 209.8 | 207.4 | 207.4 | 145.1 | 145.1 | 146.3 | 146.6 | 144.2 | 144.8 | 212.9 |
| 13 | 53.6 | 52.3 | 141.9 | 38.5 | 39.2 | 116.5 | 116.8 | 133.9 | 130.7 | 128.8 | 134.6 | 81.6 |
| 14 | 157.1 | 156.7 | 47.2 | 45.1 | 44.5 | 41.4 | 43.4 | 43.3 | 42.7 | 45.6 | 42.6 | 45.5 |
| 15 | 119.9 | 118.7 | 26.0 | 21.1 | 21.5 | 27.2 | 27.7 | 28.1 | 27.3 | 28.0 | 26.3 | 21.8 |
| 16 | 28.8 | 37.5 | 30.2 | 19.0 | 27.7 | 20.9 | 27.9 | 21.3 | 27.4 | 31.2 | 27.5 | 25.6 |
| 17 | 41.6 | 35.0 | 49.3 | 37.0 | 30.9 | 39.2 | 33.5 | 39.7 | 49.2 | 49.0 | 40.3 | 49.5 |
| 18 | 51.7 | 48.4 | 147.9 | 40.7 | 40.3 | 47.3 | 47.4 | 49.9 | 48.9 | 130.7 | 47.5 | 47.2 |
| 19 | 38.4 | 36.8 | 38.5 | 41.1 | 41.1 | 40.9 | 41.3 | 41.7 | 41.9 | 138.6 | 42.1 | 41.4 |
| 20 | 38.2 | 36.6 | 33.9 | 36.2 | 38.5 | 37.8 | 40.0 | 38.8 | 40.2 | 39.0 | 35.4 | 33.6 |
| 21 | 38.9 | 28.7 | 46.2 | 40.1 | 31.1 | 40.3 | 31.5 | 40.1 | 47.0 | 43.9 | 51.9 | 48.9 |
| 22 | 78.9 | 37.7 | 216.5 | 78.6 | 42.1 | 78.5 | 42.2 | 79.5 | 218.0 | 217.0 | 218.8 | 217.4 |
| 23 | 181.3 | 180.4 | 181.5 | 180.3 | 180.3 | 180.5 | 180.6 | 181.1 | 181.2 | 180.1 | 181.0 | 180.1 |
| 24 | 11.4 | 12.0 | 11.5 | 11.8 | 11.8 | 12.2 | 12.3 | 11.5 | 11.5 | 11.6 | 11.4 | 12.1 |
| 25 | 18.0 | 17.7 | 17.2 | 18.0 | 18.0 | 17.0 | 17.1 | 17.5 | 17.5 | 17.9 | 17.5 | 16.9 |
| 26 | 25.8 | 25.3 | 19.5 | 19.3 | 19.3 | 18.1 | 18.2 | 18.9 | 18.9 | 18.9 | 19.1 | 21.1 |
| 27 | 23.2 | 21.4 | 21.2 | 18.4 | 18.3 | 23.9 | 23.9 | 21.6 | 21.0 | 18.3 | 23.1 | 17.0 |
| 28 | 31.8 | 33.2 | 25.8 | 25.4 | 28.4 | 25.4 | 28.8 | 25.8 | 21.7 | 23.7 | 22.2 | 26.5 |
| 29 | 24.2 | 23.3 | 21.9 | 16.8 | 17.1 | 17.0 | 17.2 | 16.9 | 16.5 | 19.6 | 32.1 | 31.3 |
| 30 | 22.1 | 22.1 | 20.9 | 20.5 | 20.7 | 21.2 | 21.4 | 21.2 | 21.2 | 20.1 | 25.4 | 28.5 |
| C̲H3O– | 52.4 | 52.4 |
a
Assignments were made by a combination of 1D and 2D NMR experiments.
b
Measured in CD3OD.
c
Measured in C5D5N.