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| No. | Reaction time (h) | d(−) (nm) | Polydispersity index (%) |
|---|---|---|---|
| 1 | 0.5 | 232.3 | 0.24 |
| 2 | 1 | 295.5 | 0.23 |
| 3 | 2 | 328.6 | 0.25 |
| 4 | 4 | 430.3 | 0.26 |
| 5 | 6 | 498.6 | 0.29 |
| 6 | 8 | 513.2 | 0.31 |
| 7 | 10 | 560.3 | 0.34 |
| 8 | 12 | 590.8 | 0.35 |
| 9 | 14 | 612.7 | 0.40 |
