13C NMR data for compounds 1–6 (δ in ppm)a.
No. | 1 | 2 | 3 | 4 | 5 | 6 |
---|---|---|---|---|---|---|
1 | 208.4, C | 210.1, C | 212.4, C | 210.1, C | 212.7, C | 201.3, C |
2 | 75.7, CH | 41.2, CH2 | 42.5, CH2 | 41.9, CH2 | 42.6, CH2 | 40.5, CH2 |
3 | 30.8, CH2 | 21.5, CH2 | 22.7, CH2 | 22.6, CH2 | 22.6, CH2 | 19.6, CH2 |
4 | 29.7, CH2 | 31.6, CH2 | 30.7, CH2 | 32.2, CH2 | 31.4, CH2 | 31.7, CH2 |
5 | 74.7, CH | 74.5, CH | 74.4, CH | 79.9, CH | 74.9, CH | 76.9, CH |
6 | 57.5, CH | 59.5, CH | 57.3, CH | 62.1, CH | 55.5, CH | 141.8, C |
7 | 66.9, CH | 66.7, CH | 67.6, CH | 72.1, CH | 64.3, CH | 135.7, CH |
8 | 73.2, CH | 73.5, CH | 69.7, CH | 76.3, CH | 36.1, CH2 | 68.7, CH |
9 | 76.4, CH | 76.4, CH | 77.1, CH | 80.8, CH | 73.5, CH | 79.7, CH |
10 | 35.2, CH2 | 35.2, CH2 | 35.3, CH2 | 35.1, CH2 | 39.4, CH2 | 35.7, CH2 |
11 | 19.6, CH2 | 19.6, CH2 | 19.3, CH2 | 19.6, CH2 | 19.5, CH2 | 19.8, CH2 |
12 | 14.5, CH3 | 14.5, CH3 | 14.5, CH3 | 14.4, CH3 | 14.5, CH3 | 14.4, CH3 |
Measured at 100 MHz in methanol-d4.