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. 2020 Jun 12;10(38):22730–22741. doi: 10.1039/d0ra02775h

1H and 13C spectral data of compound 2 (600 MHz and 150 MHz, respectively, DMSO-d6).

No. δ H (m, J in Hz) δ C
1 1.17, 2.05 (m) 44.62
2 3.91 (br s) 70.11
3 3.73 (br s) 74.65
4 52.30
5 1.41 (t) 51.22
6 1.02, 1.47 (m) 20.68
7 1.19, 1.76 (m) 35.38
8 41.97
9 1.48 (br s) 50.80
10 39.20
11 1.16, 1.51 (m) 22.14
12 1.36, 2.15 (m) 33.97
13 69.12
14 52.75
15 1.65, 1.78 (m) 26.54
16 1.86, 2.60 (m) 24.93
17 48.63
18 1.72 (m) 41.38
19 1.22, 1.39 (m) 36.05
20 33.12
21 1.18, 2.32 (m) 44.35
22 3.95 (br s) 69.81
23 179.16
24 1.14 (s) 12.46
25 1.11 (s) 17.49
26 0.83 (s) 18.15
27 1.20 (s) 24.99
28 177.46
29 0.86 (s) 32.44
30 0.69 (s) 24.43