1H and 13C spectral data of compound 2 (600 MHz and 150 MHz, respectively, DMSO-d6).
No. | δ H (m, J in Hz) | δ C |
---|---|---|
1 | 1.17, 2.05 (m) | 44.62 |
2 | 3.91 (br s) | 70.11 |
3 | 3.73 (br s) | 74.65 |
4 | — | 52.30 |
5 | 1.41 (t) | 51.22 |
6 | 1.02, 1.47 (m) | 20.68 |
7 | 1.19, 1.76 (m) | 35.38 |
8 | — | 41.97 |
9 | 1.48 (br s) | 50.80 |
10 | — | 39.20 |
11 | 1.16, 1.51 (m) | 22.14 |
12 | 1.36, 2.15 (m) | 33.97 |
13 | — | 69.12 |
14 | — | 52.75 |
15 | 1.65, 1.78 (m) | 26.54 |
16 | 1.86, 2.60 (m) | 24.93 |
17 | — | 48.63 |
18 | 1.72 (m) | 41.38 |
19 | 1.22, 1.39 (m) | 36.05 |
20 | — | 33.12 |
21 | 1.18, 2.32 (m) | 44.35 |
22 | 3.95 (br s) | 69.81 |
23 | — | 179.16 |
24 | 1.14 (s) | 12.46 |
25 | 1.11 (s) | 17.49 |
26 | 0.83 (s) | 18.15 |
27 | 1.20 (s) | 24.99 |
28 | — | 177.46 |
29 | 0.86 (s) | 32.44 |
30 | 0.69 (s) | 24.43 |