1H and 13C NMR data of 1 (CDCl3).
| Position | δ C, type | δ H, mult. (J in Hz) |
|---|---|---|
| 1 | 86.2, C | |
| 2 | 160.3, C | |
| 3 | 128.7, C | |
| 4 | 171.9, C | |
| 4a | 143.7, C | |
| 6 | 164.4, C | |
| 6a | 100.9, C | |
| 7 | 164.7, C | |
| 8 | 101.7, CH | 6.62, d (2.4) |
| 9 | 166.6, C | |
| 10 | 104.7, CH | 7.20, d (2.4) |
| 10a | 134.2, C | |
| 10b | 121.7, C | |
| 1-CH3 | 26.2, CH3 | 1.86, s |
| 3-OCH3 | 60.9, CH3 | 3.83, s |
| 7-OH | 11.41, s | |
| 9-OCH3 | 55.9, CH3 | 3.91, s |
| 1′ | 97.3, CH | 5.65, t (5.6) |
| 2′ | 30.7, CH2 | 2.23, m |
| 1.81, m | ||
| 3′ | 25.4, CH2 | 2.11, m |
| 4′ | 48.8, CH2 | 3.61, m |