Powder X-ray diffraction crystallographic data for Ti–S nanostructures.

Chemical formula	TiS3	TiS2
Annealed temperature	400 °C to 550 °C	600 °C to 650 °C
Crystal system	Monoclinic	Hexagonal
a (Å)	5.02	3.39
b (Å)	3.46	3.39
c (Å)	8.79	5.66
α (degree)	90	90
β (degree)	97.73	90
γ (degree)	90	120
Cell volume V (Å3)	151.69	56.63
Space group	P2̄m1	P3̄m1
Radiation type wavelength (Å)	Cu Kα 1.5418	Cu Kα 1.5418
Profile range (°2θ)	5 to 80	5 to 80