Procedures of the nano/microcapsule synthesis with different processing parameters.

Sample	Silica nanoparticle dispersion [g]	PPG–TDI [g]	IPDI [g]	Agitation rate [rpm]	Yield [%]	Core content [wt%]	Content of silica nanoparticles [wt%]	Mean diameter [nm]
1	30	1.5	3	3000	62	28	10	1106
2	30	1.5	3	6000	45	29	18	848
3	30	1.5	3	9000	49	33	25	674
4	30	1.5	3	12 000	64	39	27	468
5	30	0.5	4	9000	58	32	21	1023
6	30	1	3.5	9000	63	44	26	865
7	30	2	2.5	9000	53	34	28	758
8	15	1.5	3	9000	47	31	10	655
9	45	1.5	3	9000	40	29	37	891