Results of XPS analysis combining the chemical state of elements present on the surface of the Ti3C2 MXene.
Name | Peak BE | At% | SF | Peak BE (−0.9 eV) | Chemical bonds |
---|---|---|---|---|---|
Ti 2p3 | 460.3 | 3.6 | 5.22 | 459.4 | Ti–O (TiO2) |
Ti 2p3 | 454.8 | 2.2 | 5.22 | 453.9 | Ti–C |
Ti 2p3 | 455.8 | 5.3 | 5.22 | 454.9 | Ti–O |
Ti 2p3 | 457.3 | 4.5 | 5.22 | 456.4 | Ti–O (amorphous TiO2) |
C 1s | 285.0 | 33.6 | 1 | 284.1 | C–C |
C 1s | 281.8 | 9.0 | 1 | 280.9 | Ti–C |
C 1s | 286.6 | 6.4 | 1 | 285.7 | C–O |
C 1s | 288.9 | 2.4 | 1 | 288.0 | C O (O C–OH) |
O 1s | 533.8 | 5.3 | 2.93 | 532.9 | C–O |
O 1s | 531.9 | 6.2 | 2.93 | 531.0 | Ti–O |
O 1s | 530.5 | 4.6 | 2.93 | 529.6 | C O |
O 1s | 535.7 | 1.1 | 2.93 | 534.8 | — |
F 1s | 685.4 | 9.5 | 4.43 | 684.5 | Al–F (AlF3) |
F 1s | 687.3 | 2.9 | 4.43 | 686.4 | Al–F (AlF3) |
F 1s | 689.4 | 0.7 | 4.43 | 688.5 | C–F |
Al 2p | 76.3 | 1.7 | 0.537 | 75.4 | Al–F (AlF3) |
Al 2p | 78.4 | 0.6 | 0.537 | 77.5 | Al–F (AlF3) |
Al 2p | 73.8 | 0.7 | 0.537 | 72.9 | Al–O (Al2O3) |