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. 2019 Jan 30;9(8):4092–4105. doi: 10.1039/c8ra07633b

Results of XPS analysis combining the chemical state of elements present on the surface of the Ti3C2 MXene.

Name Peak BE At% SF Peak BE (−0.9 eV) Chemical bonds
Ti 2p3 460.3 3.6 5.22 459.4 Ti–O (TiO2)
Ti 2p3 454.8 2.2 5.22 453.9 Ti–C
Ti 2p3 455.8 5.3 5.22 454.9 Ti–O
Ti 2p3 457.3 4.5 5.22 456.4 Ti–O (amorphous TiO2)
C 1s 285.0 33.6 1 284.1 C–C
C 1s 281.8 9.0 1 280.9 Ti–C
C 1s 286.6 6.4 1 285.7 C–O
C 1s 288.9 2.4 1 288.0 C Created by potrace 1.16, written by Peter Selinger 2001-2019 O (O Created by potrace 1.16, written by Peter Selinger 2001-2019 C–OH)
O 1s 533.8 5.3 2.93 532.9 C–O
O 1s 531.9 6.2 2.93 531.0 Ti–O
O 1s 530.5 4.6 2.93 529.6 C Created by potrace 1.16, written by Peter Selinger 2001-2019 O
O 1s 535.7 1.1 2.93 534.8
F 1s 685.4 9.5 4.43 684.5 Al–F (AlF3)
F 1s 687.3 2.9 4.43 686.4 Al–F (AlF3)
F 1s 689.4 0.7 4.43 688.5 C–F
Al 2p 76.3 1.7 0.537 75.4 Al–F (AlF3)
Al 2p 78.4 0.6 0.537 77.5 Al–F (AlF3)
Al 2p 73.8 0.7 0.537 72.9 Al–O (Al2O3)