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. 2019 Feb 12;9(9):5158–5163. doi: 10.1039/c9ra00653b

Effect of catalyst loading on synthesis of 2,4,6-triphenylpyridinea.

Entry Catalyst loading (mol%) Yieldb (%)
1 None 21
2 0.1 43
3 0.5 79
4 1 93
5 1.5 93
a

Reaction condition: benzaldehyde (1 mmol), acetophenone (2 mmol), ammonium acetate (1.5 mmol), HNTf2 catalyst at 80 °C for 50 min under solvent-free conditions.

b

Isolated yield.