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. 2019 Feb 12;9(10):5394–5401. doi: 10.1039/c9ra00511k

Comparison of different sample preconcentrations and detection methods for the determination of SA.

Application Pretreatment Detection method Solvent volumed (mL) LOD (μg mL−1) LOQ (μg mL−1) Linear range (μg mL−1) Ref.
MFGMa HPLC 8 mL 10.0 21.0 50–500 29
Infant formulas Spectrophotometric 100 mL 0.29 mg L−1 0.97 mg L−1 6–150 32
Biological samples Scanning potentiostat 20 μL 10 μmol mL−1 33
Human serum UCSHDb HPLC-MS/MS 1.08 ng mL−1 3.59 ng mL−1 0.5–16 μmol mL−1 15
Human serum DSPEc HPLC 2 mL 0.11 ng mL−1 0.36 ng mL−1 10–1000 pmol L−1 34
Rabbit serum B-MhMIPs HPLC 10 mL 0.025 0.083 0.5–10 This work
a

Yak milk fat globule membrane.

b

Ultrasonic-assisted closed in-syringe hydrolysis and derivatization.

c

Dispersive solid phase extraction.

d

Organic solvent volume in the pretreatment step.