Comparison of different sample preconcentrations and detection methods for the determination of SA.
Application | Pretreatment | Detection method | Solvent volumed (mL) | LOD (μg mL−1) | LOQ (μg mL−1) | Linear range (μg mL−1) | Ref. |
---|---|---|---|---|---|---|---|
MFGMa | — | HPLC | 8 mL | 10.0 | 21.0 | 50–500 | 29 |
Infant formulas | — | Spectrophotometric | 100 mL | 0.29 mg L−1 | 0.97 mg L−1 | 6–150 | 32 |
Biological samples | — | Scanning potentiostat | 20 μL | 10 μmol mL−1 | — | — | 33 |
Human serum | UCSHDb | HPLC-MS/MS | — | 1.08 ng mL−1 | 3.59 ng mL−1 | 0.5–16 μmol mL−1 | 15 |
Human serum | DSPEc | HPLC | 2 mL | 0.11 ng mL−1 | 0.36 ng mL−1 | 10–1000 pmol L−1 | 34 |
Rabbit serum | B-MhMIPs | HPLC | 10 mL | 0.025 | 0.083 | 0.5–10 | This work |
Yak milk fat globule membrane.
Ultrasonic-assisted closed in-syringe hydrolysis and derivatization.
Dispersive solid phase extraction.
Organic solvent volume in the pretreatment step.