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. 2019 Jan 11;9(3):1491–1500. doi: 10.1039/c8ra09067j

NMR data of compound 1a.

Position 1a 1b
δ C, type δ H (J in Hz) δ C, type δ H (J in Hz)
1/1′ 179.5, C 179.5, C
2/2′ 159.0, C 159.0, C
3/3′ 121.2, C 121.2, C
4/4′ 188.3, C 188.3, C
5/5′ 145.4, C 145.4, C
6/6′ 139.8, C 139.8, C
7/7′ 152.8, C 152.8, C
8/8′ 102.5, CH 7.17, s 102.5, CH 7.17, s
9/9′ 127.2, C 127.2, C
10/10′ 112.5, C 112.5, C
11 120.4, C 120.4, C
12 43.5, CH2 3.03, s 43.5, CH2 3.03, s
13 169.9, C 169.9, C
14 24.8, CH3 1.88, s 24.8, CH3 1.88, s
15 61.6, CH3 4.10, s 61.6, CH3 4.09, s
11′ 120.1, C 120.1, C
12′ 43.3, CH2 3.08, s 43.3, CH2 3.08, s
13′ 168.5, C 168.5, C
14′ 25.1, CH3 1.86, s 25.1, CH3 1.86, s
15′ 61.6, CH3 4.09, s 61.6, CH3 4.09, s
16′ 52.5, CH3 3.68, s 52.5, CH3 3.68, s
a

Measured in CDCl3–CD3OD (2 : 1) (1H at 600 MHz and 13C at 150 MHz).