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. 2019 Jan 11;9(3):1491–1500. doi: 10.1039/c8ra09067j

NMR data of compound 2a.

Position 2a 2b
δ C,b type δ H (J in Hz) δ C,b type δ H (J in Hz)
1/1′ 179.1, C 179.1, C
2/2′ 158.6, C 158.6, C
3/3′ n.d.c n.d.c
4/4′ 188.3, C 188.3, C
5/5′ 145.5, C 145.5, C
6/6′ 139.1, C 139.1, C
7/7′ 152.1, C 152.1, C
8/8′ 102.0, CH 7.21, s 102.0, CH 7.20, s
9/9′ 127.1, C 127.1, C
10/10′ 112.2, C 112.2, C
11/11′ 119.2, C 119.2, C
12/12′ 42.9, CH2 3.12, s 42.9, CH2 3.10, s
13/13′ 171.4, C 171.4, C
14/14′ 24.6, CH3 1.91, s 24.6, CH3 1.88, s
15/15′ 61.2, CH3 4.13, s 61.2, CH3 4.12, s
OH-5/OH-5′ 12.06, s 12.06, s
a

Measured in CDCl3 (1H at 600 MHz and 13C at 150 MHz).

b

Data were extracted from the HSQC and HMBC spectra.

c

n.d. = not detected.