13C NMR spectroscopic data for compounds 2–7 (δ in ppm).
| No. | 2a | 3a | 4b | 5b | 6b | 7b |
|---|---|---|---|---|---|---|
| 1 | 34.1 | 25.5 | 24.1 | 24.5 | 24.1 | 46.3 |
| 2 | 24.2 | 32.8 | 34.8 | 35.2 | 34.9 | 70.9 |
| 3 | 37.5 | 217.6 | 217.5 | 217.5 | 217.8 | 38.7 |
| 4 | 73.7 | 80.4 | 80.2 | 80.2 | 80.3 | 35.5 |
| 5 | 79.1 | 78.1 | 78.1 | 78.1 | 78.0 | 106.5 |
| 6 | 73.5 | 80.0 | 79.8 | 79.9 | 79.9 | 68.1 |
| 7 | 45.4 | 41.6 | 40.1 | 40.2 | 40.2 | 49.4 |
| 8 | 83.4 | 70.5 | 76.0 | 76.2 | 76.2 | 77.3 |
| 9 | 211.3 | 78.5 | 75.1 | 75.3 | 75.3 | 79.6 |
| 10 | 44.0 | 30.0 | 30.7 | 30.9 | 30.9 | 71.9 |
| 11 | 137.3 | 132.7 | 132.6 | 133.0 | 133.1 | 139.0 |
| 12 | 171.3 | 169.6 | 169.2 | 169.2 | 169.3 | 169.9 |
| 13 | 125.1 | 123.9 | 124.6 | 124.6 | 124.6 | 119.4 |
| 14 | 20.4 | 20.0 | 19.8 | 19.8 | 20.2 | 23.2 |
| 15 | 24.2 | 23.3 | 23.1 | 23.1 | 23.5 | 12.0 |
| 1′ | 179.0 | 176.4 | 176.4 | 176.4 | 167.1 | |
| 2′ | 35.0 | 34.0 | 33.9 | 34.0 | 127.4 | |
| 3′ | 19.2 | 18.0 | 18.0 | 18.0 | 138.2 | |
| 4′ | 19.2 | 17.9 | 17.9 | 17.9 | 19.2 | |
| 5′ | 14.6 | |||||
| 1′′ | 167.0 | 167.7 | 172.9 | 167.4 | 167.5 | 176.1 |
| 2′′ | 136.7 | 127.8 | 42.9 | 127.3 | 127.4 | 34.0 |
| 3′′ | 127.4 | 137.7 | 25.8 | 138.2 | 138.4 | 17.9 |
| 4′′ | 18.1 | 19.4 | 21.6 | 19.2 | 19.3 | 17.9 |
| 5′′ | 14.6 | 21.7 | 14.6 | 14.6 |
Measured at 150 MHz in methanol-d4.
Measured at 125 MHz in methanol-d4.