| 6 |
2.61 dd (15.0, 6.6); 2.19 d (16.2) |
2.61 dd (15.0, 6.6); 2.19 d (16.2) |
2.29–2.39 m |
2.68 dd (14.4, 6.6); 1.80 d (13.8) |
2.57–2.64 m; 1.77–1.84 m |
| 7 |
1.73–1.81 m |
1.73–1.81 m |
1.96–2.03 m |
2.05–2.13 m |
2.05–2.10 m |
| 12/16 |
7.56 d (7.2) |
7.56 d (7.2) |
7.58 d (8.4) |
7.31 m |
7.33 m |
| 13/15 |
7.38 t (7.8) |
7.38 t (7.8) |
7.26 t (7.8) |
7.31 m |
7.33 m |
| 14 |
7.43 t (7.8) |
7.43 t (7.8) |
7.39 t (7.8) |
7.43 m |
7.46 m |
| 17 |
2.99 dd (16.2, 6.6); 2.39–2.47 m |
2.89–2.96 m; 2.39–2.47 m |
5.07 d (2.4) |
3.44 dd (14.0, 11.4); 1.64 dd (15.0, 3.0) |
3.30 dd (15.0, 9.0); 1.74–1.82 m |
| 18 |
5.84 t (6.6) |
5.79 dd (6.6, 3.6) |
3.92 d (2.4) |
4.94 dd (11.4, 3.0) |
5.86–5.92 m |
| 20 |
|
|
1.26 s |
1.19 s |
|
| 21 |
|
|
1.33 s |
1.20 s |
|
| 22 |
2.20–2.29 m; 2.04–2.14 m |
2.20–2.29 m; 2.04–2.14 m |
2.14–2.22 m; 2.04–2.11 m |
2.28 dd (14.4, 9.6); 1.85 dd (14.4, 4.2) |
2.28 dd (14.4, 9.6); 1.77–1.84 m |
| 23 |
2.36–2.44 m |
2.36–2.44 m |
2.50–2.57 m |
2.57–2.65 m |
2.58–2.66 m |
| 25 |
1.69 s |
1.70 s |
1.72 s |
1.56 s |
1.50 s |
| 26 |
4.73 s |
4.73 s |
4.79 s; 4.81 s |
4.70 s; 4.62 s |
4.57 br s; 4.70 br s |
| 27 |
2.00–2.07 m; 1.87–1.95 m |
2.00–2.07 m; 1.87–1.95 m |
2.10–2.16 m; 2.01–2.07 m |
2.04–2.14 m |
2.01–2.07 m |
| 28 |
5.07 t (6.6) |
5.07 t (6.6) |
5.03–5.09 m |
5.03 t (6.6) |
5.00 t (6.6) |
| 30 |
1.55 s |
1.56 s |
1.59 s |
1.62 s |
1.61 s |
| 31 |
1.64 s |
1.64 s |
1.65 s |
1.69 s |
1.68 s |
| 32 |
1.87–2.02 m |
1.87–2.02 m |
2.04–2.10 m; 1.97–2.04 m |
2.31–2.40 m; 1.45–1.55 m |
2.33 dd (13.8, 7.2); 1.45–1.52 m |
| 33 |
2.41–2.48 m |
2.50–2.55 m |
2.46–2.53 m |
2.72 t (10.2) |
2.58–2.66 m |
| 35 |
1.58 s |
1.70 s |
1.37 s |
1.33 s |
1.32 s |
| 36 |
1.46 s |
1.50 s |
1.34 s |
1.20 s |
1.25 s |
| 37 |
1.21 s |
1.19 s |
1.44 s |
1.35 s |
1.39 s |
| 38 |
1.47 s |
1.47 s |
1.39 s |
1.48 s |
1.44 s |
| OH |
|
|
4.75 s |
|
|