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. 2019 May 21;9(28):15941–15948. doi: 10.1039/c9ra02546d

Textural properties, density of –SO3H groups and catalytic activity of reused SO3H-OMC(s)-6-160 catalyst samples.

Reuse times of catalyst samples Specific surface area (m2 g−1) Pore volume (cm3 g−1) Density of –SO3H groups (mmol g−1) FFAs conv. (%)
S total S micro S meso V total V micro V meso
Fresh 537 116 421 0.85 0.09 0.76 2.32 93.8
First reuse 517 112 405 0.81 0.09 0.72 2.18 90.1
Second reuse 496 113 386 0.77 0.08 0.69 2.07 87.3
Third reuse 487 110 377 0.76 0.08 0.68 2.02 85.9
Fourth reuse 485 113 372 0.75 0.08 0.67 1.98 85.5
Fifth reuse 484 108 378 0.75 0.08 0.67 1.97 85.2