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. 2019 Jun 12;9(32):18547–18558. doi: 10.1039/c9ra03254a

Fig. 4. Bright-field image of multiple CoCrFeMnNi HEA NPs (a) and the respective diffraction pattern (b) proving the fcc-type structure of the NPs. In (c) a single and larger crystalline nanoparticle is shown with the respective diffraction pattern in (d). The same crystal structure is determined for small nanoparticles by the high-resolution TEM micrograph (e) and the respective fast Fourier transform (f). An inset of (e) is magnified in (g) (scale bar is 1 nm). High-resolution TEM micrograph of a large disordered NP (>100 nm) (h) and the respective diffraction pattern with diffuse streaks and reflection splitting (i).

Fig. 4