13C NMR data of 1–4 (125 MHz, δ in ppm).
1 | 2 | 3 | 4 | |
---|---|---|---|---|
1 | 43.9 | 44.2 | 43.9 | 43.9 |
2 | 24.5 | 24.5 | 24.9 | 24.0 |
3 | 29.0 | 28.9 | 29.5 | 28.6 |
4 | 66.9 | 67.1 | 68.9 | 66.3 |
5 | 30.1 | 30.9 | 30.1 | 30.0 |
6 | 44.7 | 51.6 | 55.7 | 49.5 |
7 | 35.3 | 36.4 | 44.0 | 36.1 |
8 | 141.2 | 152.9 | 177.9 | 152.0 |
9 | 127.8 | 130.8 | 139.2 | 139.6 |
10 | 106.4 | 105.9 | 104.8 | 111.4 |
11 | 118.8 | 117.5 | 117.1 | 115.4 |
12 | 129.9 | 130.5 | 130.7 | 133.0 |
13 | 75.6 | 75.8 | 76.3 | 76.2 |
14 | 138.3 | 150.2 | 152.8 | 153.9 |
15 | 143.9 | 113.6 | 108.8 | 116.4 |
16 | 102.8 | 121.3 | 125.6 | 123.7 |
17 | 120.0 | 115.4 | 121.4 | 128.9 |
18 | 109.1 | 105.4 | 67.9 | 77.5 |
19 | 59.8 | 183.9 | 83.2 | 75.6 |
20 | 62.8 | 67.4 | 65.1 | 61.8 |
21 | 168.4 | 167.0 | 169.3 | 168.0 |
22 | 172.8 | 172.3 | 173.4 | 171.7 |
23 | 28.5 | 26.4 | 19.4 | 22.4 |
24 | 22.3 | 19.2 | 22.6 | 13.0 |
25 | 27.4 | 27.3 | 28.0 | 27.4 |
26 | 27.4 | 27.5 | 28.2 | 27.4 |
OMe | 56.9 | 60.1 | 59.5 |