Difenoconazole and propiconazole recoveries in leaf, whole fruit and soil samples (n = 5).

Compound	Matrix	Spiked level (mg kg−1)	Recovery (%), intraday RSD (%, n = 5)						Inter-day RSD (%, n = 15)
			Day 1		Day 2		Day 3
Difenoconazole	Leaf	0.02	93.1	4.9	91.4	7.0	93.7	4.9	1.2
		0.2	88.3	4.8	88.9	3.2	90.8	1.7	1.3
		2	80.6	5.2	81.2	4.2	83.9	5.4	1.8
		20	84.7	5.8	84.9	5.1	86.7	4.5	1.1
	Whole fruit	0.02	90.9	5.4	88.2	5.8	90.7	6.2	1.5
		0.2	86.2	4.7	85.8	2.6	88.4	3.5	1.4
		2	84.3	2.9	83.6	2.4	82.9	3.4	0.7
	Soil	0.02	93.3	3.6	94.9	1.6	93.2	3.7	0.9
		0.2	82.0	4.0	81.4	4.1	83.7	4.1	1.2
		2	76.7	1.7	78.3	1.0	83.2	3.1	3.4
		20	83.4	4.4	83.9	4.6	90.2	4.3	3.8
Propiconazole	Leaf	0.02	90.8	3.8	91.5	5.8	92.1	4.9	0.6
		0.2	88.0	2.8	88.9	2.6	85.7	5.1	1.6
		2	81.4	2.9	82.7	3.2	83.5	4.5	1.1
		20	79.8	0.9	80.9	2.1	83.4	3.8	1.8
	Whole fruit	0.02	91.2	2.9	91.7	3.2	92.4	2.9	0.6
		0.2	84.6	2.0	86.3	2.2	87.7	2.3	1.6
		2	85.7	4.7	84.4	6.0	85.6	5.1	0.7
	Soil	0.02	93.5	3.2	93.6	3.1	94.8	1.1	0.7
		0.2	90.0	4.1	90.9	2.6	83.8	3.9	3.9
		2	86.2	3.0	85.3	4.1	82.9	3.4	1.7
		20	79.6	3.5	82.3	4.2	84.7	7.4	2.6