GLC-MS analysis of the methylated polysaccharide.
Methylated sugars | Molar ratio | Linkage-type | Major mass fragments (m/z) |
---|---|---|---|
2,3,4-Me3-Glc | 4 | →6)-Glcp-(1→ | 39, 53, 77, 101, 112, 121, 152, 171, 204 |
2,3,4,-Me3-Glc | 1 | →6)-Glcp-(1→ | 77, 101, 112, 135, 171, 189, 204 |
2,3,4-Me3-Glc | 2 | →6)-Glcp-(1→ | 39, 53, 77, 93, 101, 112, 121, 152 |
2,3,4,-Me3-Glc | 1 | →6)-Glcp-(1→ | 39, 53, 77, 101, 121, 135, 161, 171, 189 |
2,3,4,6-Me4-Glc | 1 | Glcp-(1→ | 39, 53, 77, 101, 112, 121, 135, 189, 204 |