13C NMR spectroscopic data of compounds 1–5.
| 1a | 2b | 3c | 4d | 5b | |
|---|---|---|---|---|---|
| 1 | 129.5 | 131.3 | 128.0 | 121.2 | 133.3 |
| 2 | 110.3 | 113.4 | 116.9 | 115.1 | 107.7 |
| 3 | 146.7 | 146.6 | 153.2 | 148.1 | 151.9 |
| 4 | 150.1 | 142.9 | 145.8 | 145.4 | 144.9 |
| 5 | 113.7 | 115.8 | 111.0 | 112.3 | 112.8 |
| 6 | 123.3 | 132.1 | 141.1 | 138.3 | 121.2 |
| 7 | 202.9 | 36.2 | 190.9 | 66.9 | 121.4 |
| 8 | 42.8 | 48.9 | 211.6 | 36.6 | 145.4 |
| 9 | 11.6 | 16.5 | 28.8 | 9.9 | 19.8 |
| 1′ | 132.5 | 130.8 | 134.9 | 137.6 | 132.6 |
| 2′ | 111.3 | 111.2 | 113.0 | 112.2 | 109.3 |
| 3′ | 147.1 | 147.6 | 148.3 | 148.1 | 146.5 |
| 4′ | 141.0 | 150.4 | 146.1 | 145.4 | 144.7 |
| 5′ | 124.3 | 113.6 | 115.8 | 115.1 | 114.2 |
| 6′ | 123.8 | 126.5 | 121.0 | 121.4 | 119.5 |
| 7′ | 41.5 | 196.3 | 46.6 | 56.7 | 200.6 |
| 8′ | 37.7 | 212.6 | 52.0 | 36.6 | 55.0 |
| 9′ | 15.5 | 29.1 | 16.8 | 12.1 | 22.0 |
| OCH3-3 | 56.0 | 56.1 | 56.5 | 56.2 | 56.0 |
| OCH3-3′ | 56.1 | 56.2 | 56.3 | 56.2 | 55.8 |
13C NMR data (δ) were measured in chloroform-d at 75 MHz.
13C NMR data (δ) were measured in chloroform-d at 100 MHz.
13C NMR data (δ) were measured in acetone-d6 at 100 MHz.
13C NMR data (δ) were measured in acetone-d6 at 75 MHz.