Results obtained by the proposed methods for the determination of l-ORN using NBD-Cl in authentic form and in pharmaceutical preparation compared to the reported method11.
Parameter | Proposed method | Reported method11 | Now Foods® capsules |
---|---|---|---|
Meana | 99.84 | 98.69 | 100.9 |
±SD | 1.491 | 1.56 | 1.10 |
RSD | 1.494 | 1.58 | 1.09 |
V | 2.22 | 2.13 | 1.21 |
n | 7 | 3 | 6 |
±SE | 0.564 | 0.400 | 0.450 |
t-value | 1.083 (2.262)a | ||
F | 1.04 (19.3)b |
Average of 3 determinations; a and b are the tabulated t-values and F-ratios at p = 0.05.