Table 1. Data-collection and refinement statistics.
Values for highest resolution shells are given in parentheses.
| I923.40N–UK-432097 | |
|---|---|
| Data collection | |
| Space group | C2 |
| Cell dimensions | |
| a, b, c (Å) | 71.23, 175.70, 112.70 |
| α, β, γ (°) | 90, 91.21, 90 |
| Resolution (Å) | 47.43–3.80 (3.94–3.80) |
| Reflections (total/unique) | 594392/13682 |
| R p.i.m. | 0.14 (5.75) |
| CC1/2 † | 0.99 (0.69) |
| 〈I/σ(I)〉 | 10.46 (1.52) |
| Completeness (%) | 99.9 (100) |
| Redundancy | 43.4 (41.9) |
| Refinement | |
| R work/R free | 0.284/0.316 |
| R.m.s.d. | |
| Bond lengths (Å) | 0.004 |
| Bond angles (°) | 0.641 |
| Ramachandran plot (%)‡ | 93.5/6.1/0.4 |
| PDB ID | 7ezc |
†
CC1/2 = Pearson’s correlation coefficient between average intensities of random half data sets for each unique reflection.
‡
Residues in favored, accepted and outlier regions of the Ramachandran plot as reported by MolProbity (Williams et al., 2018 ▸).