Skip to main content
. 2022 Apr 5;78(Pt 5):473–476. doi: 10.1107/S2056989022003437

Table 2. Experimental details.

Crystal data
Chemical formula [Cu(C16H12N3O2)Cl]·H2O
M r 395.29
Crystal system, space group Monoclinic, P21/n
Temperature (K) 100
a, b, c (Å) 3.7711 (4), 26.451 (3), 15.0864 (15)
β (°) 97.100 (2)
V3) 1493.3 (3)
Z 4
Radiation type Mo Kα
μ (mm−1) 1.66
Crystal size (mm) 0.44 × 0.09 × 0.02
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Krause et al., 2015)
T min, T max 0.629, 0.745
No. of measured, independent and observed [I > 2σ(I)] reflections 8133, 2746, 2132
R int 0.049
(sin θ/λ)max−1) 0.602
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.036, 0.081, 1.04
No. of reflections 2746
No. of parameters 230
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
Δρmax, Δρmin (e Å−3) 0.42, −0.41

Computer programs: APEX2 and SAINT (Bruker, 2014), SHELXT2014/5 (Sheldrick, 2015a ), SHELXL2017/1 (Sheldrick, 2015b ), and SHELXTL (Sheldrick, 2008).