| Crystal data |
| Chemical formula |
(NH4)2[Zn(C3H7NO)(H2O)5]2[V10O28]·4H2O |
|
M
r
|
1522.64 |
| Crystal system, space group |
Monoclinic, P21/n
|
| Temperature (K) |
120 |
|
a, b, c (Å) |
15.5436 (6), 8.6538 (4), 16.7362 (7) |
| β (°) |
108.628 (1) |
|
V (Å3) |
2133.27 (16) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
3.31 |
| Crystal size (mm) |
0.49 × 0.23 × 0.10 |
| |
| Data collection |
| Diffractometer |
Nonius KappaCCD with Buker APEXII detector |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.57, 0.73 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
29908, 4901, 4354 |
|
R
int
|
0.033 |
| (sin θ/λ)max (Å−1) |
0.650 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.023, 0.056, 1.06 |
| No. of reflections |
4901 |
| No. of parameters |
372 |
| No. of restraints |
6 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.36, −0.62 |
