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. 2022 Apr 22;78(Pt 5):506–509. doi: 10.1107/S2056989022004200
Bruker APEXII CCD diffractometer 6730 independent reflections
Radiation source: fine-focus sealed tube 6601 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.024
Detector resolution: 8.3660 pixels mm-1 θmax = 27.1°, θmin = 1.4°
phi and ω scans h = −12→12
Absorption correction: multi-scan (SADABS; Bruker, 2014) k = −36→36
Tmin = 0.690, Tmax = 0.746 l = −14→14
39572 measured reflections