| Bruker APEXII CCD diffractometer | 6730 independent reflections |
| Radiation source: fine-focus sealed tube | 6601 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.024 |
| Detector resolution: 8.3660 pixels mm-1 | θmax = 27.1°, θmin = 1.4° |
| phi and ω scans | h = −12→12 |
| Absorption correction: multi-scan (SADABS; Bruker, 2014) | k = −36→36 |
| Tmin = 0.690, Tmax = 0.746 | l = −14→14 |
| 39572 measured reflections |