Refinement on F2 | Hydrogen site location: mixed |
Least-squares matrix: full | H atoms treated by a mixture of independent and constrained refinement |
R[F2 > 2σ(F2)] = 0.074 | w = 1/[σ2(Fo2) + (0.0554P)2 + 0.9198P] where P = (Fo2 + 2Fc2)/3 |
wR(F2) = 0.169 | (Δ/σ)max < 0.001 |
S = 1.00 | Δρmax = 0.27 e Å−3 |
6715 reflections | Δρmin = −0.18 e Å−3 |
507 parameters | Extinction correction: SHELXL2018/3 (Sheldrick 2015b), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
45 restraints | Extinction coefficient: 0.0029 (4) |
0 constraints |