O1—N3 | 1.222 (3) | C8—H8B | 0.97 |
O2—N3 | 1.217 (3) | C9—C10 | 1.516 (3) |
N1—C1 | 1.391 (3) | C9—H9A | 0.97 |
N1—C7 | 1.474 (3) | C9—H9B | 0.97 |
N1—C10 | 1.477 (3) | C10—H10A | 0.97 |
N2—C9 | 1.476 (4) | C10—H10B | 0.97 |
N2—C8 | 1.490 (3) | Br1—C14 | 1.906 (2) |
N2—H21 | 0.850 (17) | O3—C17 | 1.264 (3) |
N2—H22 | 0.833 (18) | O4—C17 | 1.257 (3) |
N3—C4 | 1.454 (3) | C11—C16 | 1.388 (3) |
C1—C2 | 1.405 (3) | C11—C12 | 1.391 (3) |
C1—C6 | 1.410 (3) | C11—C17 | 1.506 (3) |
C2—C3 | 1.376 (3) | C12—C13 | 1.385 (3) |
C2—H2 | 0.93 | C12—H12 | 0.93 |
C3—C4 | 1.377 (4) | C13—C14 | 1.374 (4) |
C3—H3 | 0.93 | C13—H13 | 0.93 |
C4—C5 | 1.378 (4) | C14—C15 | 1.378 (4) |
C5—C6 | 1.372 (3) | C15—C16 | 1.382 (3) |
C5—H5 | 0.93 | C15—H15 | 0.93 |
C6—H6 | 0.93 | C16—H16 | 0.93 |
C7—C8 | 1.502 (3) | O5—H1W | 0.802 (17) |
C7—H7A | 0.97 | O5—H2W | 0.802 (17) |
C7—H7B | 0.97 | O6—H4W | 0.823 (17) |
C8—H8A | 0.97 | O6—H3W | 0.778 (18) |
C1—N1—C7 | 117.46 (19) | N2—C8—H8B | 109.4 |
C1—N1—C10 | 117.30 (18) | C7—C8—H8B | 109.4 |
C7—N1—C10 | 112.08 (19) | H8A—C8—H8B | 108 |
C9—N2—C8 | 109.8 (2) | N2—C9—C10 | 110.3 (2) |
C9—N2—H21 | 113 (2) | N2—C9—H9A | 109.6 |
C8—N2—H21 | 110 (2) | C10—C9—H9A | 109.6 |
C9—N2—H22 | 115 (2) | N2—C9—H9B | 109.6 |
C8—N2—H22 | 106 (2) | C10—C9—H9B | 109.6 |
H21—N2—H22 | 102 (3) | H9A—C9—H9B | 108.1 |
O2—N3—O1 | 122.4 (2) | N1—C10—C9 | 111.3 (2) |
O2—N3—C4 | 118.8 (2) | N1—C10—H10A | 109.4 |
O1—N3—C4 | 118.8 (2) | C9—C10—H10A | 109.4 |
N1—C1—C2 | 121.5 (2) | N1—C10—H10B | 109.4 |
N1—C1—C6 | 121.4 (2) | C9—C10—H10B | 109.4 |
C2—C1—C6 | 117.1 (2) | H10A—C10—H10B | 108 |
C3—C2—C1 | 121.2 (2) | C16—C11—C12 | 118.6 (2) |
C3—C2—H2 | 119.4 | C16—C11—C17 | 120.5 (2) |
C1—C2—H2 | 119.4 | C12—C11—C17 | 120.9 (2) |
C2—C3—C4 | 119.9 (2) | C13—C12—C11 | 120.9 (2) |
C2—C3—H3 | 120 | C13—C12—H12 | 119.5 |
C4—C3—H3 | 120 | C11—C12—H12 | 119.5 |
C3—C4—C5 | 120.6 (2) | C14—C13—C12 | 119.0 (2) |
C3—C4—N3 | 119.2 (2) | C14—C13—H13 | 120.5 |
C5—C4—N3 | 120.2 (2) | C12—C13—H13 | 120.5 |
C6—C5—C4 | 119.8 (2) | C13—C14—C15 | 121.4 (2) |
C6—C5—H5 | 120.1 | C13—C14—Br1 | 119.7 (2) |
C4—C5—H5 | 120.1 | C15—C14—Br1 | 118.9 (2) |
C5—C6—C1 | 121.4 (2) | C14—C15—C16 | 119.2 (2) |
C5—C6—H6 | 119.3 | C14—C15—H15 | 120.4 |
C1—C6—H6 | 119.3 | C16—C15—H15 | 120.4 |
N1—C7—C8 | 111.5 (2) | C15—C16—C11 | 120.9 (2) |
N1—C7—H7A | 109.3 | C15—C16—H16 | 119.6 |
C8—C7—H7A | 109.3 | C11—C16—H16 | 119.6 |
N1—C7—H7B | 109.3 | O4—C17—O3 | 124.3 (2) |
C8—C7—H7B | 109.3 | O4—C17—C11 | 117.8 (2) |
H7A—C7—H7B | 108 | O3—C17—C11 | 117.9 (2) |
N2—C8—C7 | 111.17 (19) | H1W—O5—H2W | 108 (3) |
N2—C8—H8A | 109.4 | H4W—O6—H3W | 109 (3) |
C7—C8—H8A | 109.4 | ||
C7—N1—C1—C2 | 10.7 (3) | C9—N2—C8—C7 | 58.1 (3) |
C10—N1—C1—C2 | 148.9 (2) | N1—C7—C8—N2 | −55.1 (3) |
C7—N1—C1—C6 | −171.5 (2) | C8—N2—C9—C10 | −58.5 (3) |
C10—N1—C1—C6 | −33.3 (3) | C1—N1—C10—C9 | 165.8 (2) |
N1—C1—C2—C3 | 176.8 (2) | C7—N1—C10—C9 | −53.9 (3) |
C6—C1—C2—C3 | −1.1 (4) | N2—C9—C10—N1 | 56.8 (3) |
C1—C2—C3—C4 | 2.0 (4) | C16—C11—C12—C13 | 1.3 (3) |
C2—C3—C4—C5 | −1.6 (4) | C17—C11—C12—C13 | −179.4 (2) |
C2—C3—C4—N3 | 179.0 (2) | C11—C12—C13—C14 | −1.7 (4) |
O2—N3—C4—C3 | −174.9 (3) | C12—C13—C14—C15 | 0.4 (4) |
O1—N3—C4—C3 | 5.0 (4) | C12—C13—C14—Br1 | 179.36 (19) |
O2—N3—C4—C5 | 5.7 (4) | C13—C14—C15—C16 | 1.2 (4) |
O1—N3—C4—C5 | −174.4 (3) | Br1—C14—C15—C16 | −177.75 (18) |
C3—C4—C5—C6 | 0.5 (4) | C14—C15—C16—C11 | −1.6 (3) |
N3—C4—C5—C6 | 179.9 (2) | C12—C11—C16—C15 | 0.4 (3) |
C4—C5—C6—C1 | 0.3 (4) | C17—C11—C16—C15 | −178.9 (2) |
N1—C1—C6—C5 | −177.9 (2) | C16—C11—C17—O4 | −26.9 (3) |
C2—C1—C6—C5 | 0.0 (4) | C12—C11—C17—O4 | 153.8 (2) |
C1—N1—C7—C8 | −166.7 (2) | C16—C11—C17—O3 | 153.3 (2) |
C10—N1—C7—C8 | 53.0 (3) | C12—C11—C17—O3 | −26.0 (3) |