O1—N3 | 1.220 (3) | O6—N6 | 1.231 (4) |
O2—N3 | 1.213 (3) | O7—N6 | 1.223 (4) |
N3—C4 | 1.447 (3) | N6—C23 | 1.456 (4) |
N1—C1 | 1.384 (3) | N4—C20 | 1.378 (3) |
N1—C7 | 1.462 (3) | N4—C26 | 1.449 (3) |
N1—C10 | 1.467 (3) | N4—C29 | 1.452 (3) |
N2—C9 | 1.475 (3) | N5—C27 | 1.476 (4) |
N2—C8 | 1.481 (4) | N5—C28 | 1.486 (3) |
N2—H31N | 0.937 (19) | N5—H61N | 0.910 (19) |
N2—H32N | 0.895 (19) | N5—H62N | 0.896 (19) |
C1—C2 | 1.405 (3) | C20—C21 | 1.384 (4) |
C1—C6 | 1.412 (3) | C20—C25 | 1.391 (4) |
C2—C3 | 1.366 (4) | C21—C22 | 1.370 (4) |
C2—H2 | 0.93 | C21—H21 | 0.93 |
C3—C4 | 1.376 (4) | C22—C23 | 1.349 (4) |
C3—H3 | 0.93 | C22—H22 | 0.93 |
C4—C5 | 1.377 (4) | C23—C24 | 1.359 (5) |
C5—C6 | 1.372 (3) | C24—C25 | 1.381 (4) |
C5—H5 | 0.93 | C24—H24 | 0.93 |
C6—H6 | 0.93 | C25—H25 | 0.93 |
C7—C8 | 1.498 (3) | C26—C27 | 1.497 (4) |
C7—H7A | 0.97 | C26—H26A | 0.97 |
C7—H7B | 0.97 | C26—H26B | 0.97 |
C8—H8A | 0.97 | C27—H27A | 0.97 |
C8—H8B | 0.97 | C27—H27B | 0.97 |
C9—C10 | 1.493 (3) | C28—C29 | 1.498 (4) |
C9—H9A | 0.97 | C28—H28A | 0.97 |
C9—H9B | 0.97 | C28—H28B | 0.97 |
C10—H10A | 0.97 | C29—H29A | 0.97 |
C10—H10B | 0.97 | C29—H29B | 0.97 |
O3—C17 | 1.261 (3) | O8—C36 | 1.264 (3) |
O4—C17 | 1.253 (3) | O9—C36 | 1.252 (3) |
O5—C14 | 1.365 (3) | O10—C33 | 1.363 (3) |
O5—C18 | 1.426 (3) | O10—C37 | 1.431 (4) |
C11—C12 | 1.375 (4) | C30—C35 | 1.372 (3) |
C11—C16 | 1.383 (3) | C30—C31 | 1.387 (4) |
C11—C17 | 1.499 (4) | C30—C36 | 1.500 (4) |
C12—C13 | 1.379 (4) | C31—C32 | 1.376 (4) |
C12—H12 | 0.93 | C31—H31 | 0.93 |
C13—C14 | 1.373 (4) | C32—C33 | 1.383 (4) |
C13—H13 | 0.93 | C32—H32 | 0.93 |
C14—C15 | 1.378 (4) | C33—C34 | 1.381 (4) |
C15—C16 | 1.374 (4) | C34—C35 | 1.378 (4) |
C15—H15 | 0.93 | C34—H34 | 0.93 |
C16—H16 | 0.93 | C35—H35 | 0.93 |
C18—C19 | 1.502 (4) | C37—C38 | 1.496 (5) |
C18—H18A | 0.97 | C37—H37A | 0.97 |
C18—H18B | 0.97 | C37—H37B | 0.97 |
C19—H19A | 0.96 | C38—H38A | 0.96 |
C19—H19B | 0.96 | C38—H38B | 0.96 |
C19—H19C | 0.96 | C38—H38C | 0.96 |
O2—N3—O1 | 122.7 (3) | O7—N6—O6 | 123.5 (4) |
O2—N3—C4 | 119.3 (3) | O7—N6—C23 | 118.2 (4) |
O1—N3—C4 | 118.0 (3) | O6—N6—C23 | 118.2 (4) |
C1—N1—C7 | 118.1 (2) | C20—N4—C26 | 121.3 (2) |
C1—N1—C10 | 117.0 (2) | C20—N4—C29 | 121.3 (2) |
C7—N1—C10 | 116.3 (2) | C26—N4—C29 | 111.9 (2) |
C9—N2—C8 | 107.9 (2) | C27—N5—C28 | 110.0 (2) |
C9—N2—H31N | 110 (3) | C27—N5—H61N | 112 (3) |
C8—N2—H31N | 108 (3) | C28—N5—H61N | 110 (3) |
C9—N2—H32N | 111 (3) | C27—N5—H62N | 108 (3) |
C8—N2—H32N | 106 (3) | C28—N5—H62N | 110 (3) |
H31N—N2—H32N | 113 (4) | H61N—N5—H62N | 107 (4) |
N1—C1—C2 | 120.9 (2) | N4—C20—C21 | 121.8 (3) |
N1—C1—C6 | 122.0 (2) | N4—C20—C25 | 122.0 (3) |
C2—C1—C6 | 117.1 (2) | C21—C20—C25 | 116.2 (3) |
C3—C2—C1 | 121.3 (3) | C22—C21—C20 | 121.6 (3) |
C3—C2—H2 | 119.3 | C22—C21—H21 | 119.2 |
C1—C2—H2 | 119.3 | C20—C21—H21 | 119.2 |
C2—C3—C4 | 120.1 (3) | C23—C22—C21 | 120.9 (3) |
C2—C3—H3 | 120 | C23—C22—H22 | 119.6 |
C4—C3—H3 | 120 | C21—C22—H22 | 119.6 |
C3—C4—C5 | 120.6 (3) | C22—C23—C24 | 119.7 (3) |
C3—C4—N3 | 119.6 (3) | C22—C23—N6 | 120.8 (4) |
C5—C4—N3 | 119.8 (3) | C24—C23—N6 | 119.5 (4) |
C6—C5—C4 | 119.8 (3) | C23—C24—C25 | 119.9 (3) |
C6—C5—H5 | 120.1 | C23—C24—H24 | 120 |
C4—C5—H5 | 120.1 | C25—C24—H24 | 120 |
C5—C6—C1 | 121.2 (3) | C24—C25—C20 | 121.6 (3) |
C5—C6—H6 | 119.4 | C24—C25—H25 | 119.2 |
C1—C6—H6 | 119.4 | C20—C25—H25 | 119.2 |
N1—C7—C8 | 113.3 (2) | N4—C26—C27 | 110.5 (2) |
N1—C7—H7A | 108.9 | N4—C26—H26A | 109.5 |
C8—C7—H7A | 108.9 | C27—C26—H26A | 109.5 |
N1—C7—H7B | 108.9 | N4—C26—H26B | 109.5 |
C8—C7—H7B | 108.9 | C27—C26—H26B | 109.5 |
H7A—C7—H7B | 107.7 | H26A—C26—H26B | 108.1 |
N2—C8—C7 | 110.9 (2) | N5—C27—C26 | 111.0 (2) |
N2—C8—H8A | 109.5 | N5—C27—H27A | 109.4 |
C7—C8—H8A | 109.5 | C26—C27—H27A | 109.4 |
N2—C8—H8B | 109.5 | N5—C27—H27B | 109.4 |
C7—C8—H8B | 109.5 | C26—C27—H27B | 109.4 |
H8A—C8—H8B | 108 | H27A—C27—H27B | 108 |
N2—C9—C10 | 111.5 (2) | N5—C28—C29 | 111.1 (2) |
N2—C9—H9A | 109.3 | N5—C28—H28A | 109.4 |
C10—C9—H9A | 109.3 | C29—C28—H28A | 109.4 |
N2—C9—H9B | 109.3 | N5—C28—H28B | 109.4 |
C10—C9—H9B | 109.3 | C29—C28—H28B | 109.4 |
H9A—C9—H9B | 108 | H28A—C28—H28B | 108 |
N1—C10—C9 | 113.7 (2) | N4—C29—C28 | 111.5 (2) |
N1—C10—H10A | 108.8 | N4—C29—H29A | 109.3 |
C9—C10—H10A | 108.8 | C28—C29—H29A | 109.3 |
N1—C10—H10B | 108.8 | N4—C29—H29B | 109.3 |
C9—C10—H10B | 108.8 | C28—C29—H29B | 109.3 |
H10A—C10—H10B | 107.7 | H29A—C29—H29B | 108 |
C14—O5—C18 | 118.3 (2) | C33—O10—C37 | 118.5 (3) |
C12—C11—C16 | 117.5 (2) | C35—C30—C31 | 117.1 (3) |
C12—C11—C17 | 120.9 (2) | C35—C30—C36 | 120.9 (3) |
C16—C11—C17 | 121.6 (3) | C31—C30—C36 | 122.0 (2) |
C11—C12—C13 | 122.1 (3) | C32—C31—C30 | 121.5 (3) |
C11—C12—H12 | 119 | C32—C31—H31 | 119.2 |
C13—C12—H12 | 119 | C30—C31—H31 | 119.2 |
C14—C13—C12 | 119.5 (3) | C31—C32—C33 | 120.0 (3) |
C14—C13—H13 | 120.3 | C31—C32—H32 | 120 |
C12—C13—H13 | 120.3 | C33—C32—H32 | 120 |
O5—C14—C13 | 124.4 (3) | O10—C33—C34 | 124.5 (3) |
O5—C14—C15 | 116.1 (3) | O10—C33—C32 | 116.1 (3) |
C13—C14—C15 | 119.5 (3) | C34—C33—C32 | 119.4 (3) |
C16—C15—C14 | 120.2 (3) | C35—C34—C33 | 119.2 (3) |
C16—C15—H15 | 119.9 | C35—C34—H34 | 120.4 |
C14—C15—H15 | 119.9 | C33—C34—H34 | 120.4 |
C15—C16—C11 | 121.2 (3) | C30—C35—C34 | 122.7 (3) |
C15—C16—H16 | 119.4 | C30—C35—H35 | 118.6 |
C11—C16—H16 | 119.4 | C34—C35—H35 | 118.6 |
O4—C17—O3 | 123.5 (2) | O9—C36—O8 | 124.0 (3) |
O4—C17—C11 | 119.3 (3) | O9—C36—C30 | 118.3 (3) |
O3—C17—C11 | 117.3 (2) | O8—C36—C30 | 117.7 (3) |
O5—C18—C19 | 107.3 (3) | O10—C37—C38 | 107.4 (3) |
O5—C18—H18A | 110.3 | O10—C37—H37A | 110.2 |
C19—C18—H18A | 110.3 | C38—C37—H37A | 110.2 |
O5—C18—H18B | 110.3 | O10—C37—H37B | 110.2 |
C19—C18—H18B | 110.3 | C38—C37—H37B | 110.2 |
H18A—C18—H18B | 108.5 | H37A—C37—H37B | 108.5 |
C18—C19—H19A | 109.5 | C37—C38—H38A | 109.5 |
C18—C19—H19B | 109.5 | C37—C38—H38B | 109.5 |
H19A—C19—H19B | 109.5 | H38A—C38—H38B | 109.5 |
C18—C19—H19C | 109.5 | C37—C38—H38C | 109.5 |
H19A—C19—H19C | 109.5 | H38A—C38—H38C | 109.5 |
H19B—C19—H19C | 109.5 | H38B—C38—H38C | 109.5 |
C7—N1—C1—C2 | −173.1 (2) | C26—N4—C20—C21 | −149.7 (3) |
C10—N1—C1—C2 | −26.5 (3) | C29—N4—C20—C21 | 2.0 (4) |
C7—N1—C1—C6 | 8.5 (3) | C26—N4—C20—C25 | 33.3 (4) |
C10—N1—C1—C6 | 155.0 (2) | C29—N4—C20—C25 | −175.1 (3) |
N1—C1—C2—C3 | −177.9 (2) | N4—C20—C21—C22 | −174.3 (3) |
C6—C1—C2—C3 | 0.6 (4) | C25—C20—C21—C22 | 2.8 (5) |
C1—C2—C3—C4 | −0.7 (4) | C20—C21—C22—C23 | −1.3 (5) |
C2—C3—C4—C5 | 0.3 (4) | C21—C22—C23—C24 | −0.7 (5) |
C2—C3—C4—N3 | −178.7 (3) | C21—C22—C23—N6 | 177.8 (3) |
O2—N3—C4—C3 | −170.8 (3) | O7—N6—C23—C22 | −179.8 (3) |
O1—N3—C4—C3 | 9.6 (4) | O6—N6—C23—C22 | −3.4 (5) |
O2—N3—C4—C5 | 10.2 (4) | O7—N6—C23—C24 | −1.3 (5) |
O1—N3—C4—C5 | −169.4 (3) | O6—N6—C23—C24 | 175.1 (3) |
C3—C4—C5—C6 | 0.2 (4) | C22—C23—C24—C25 | 0.9 (5) |
N3—C4—C5—C6 | 179.2 (3) | N6—C23—C24—C25 | −177.6 (3) |
C4—C5—C6—C1 | −0.2 (4) | C23—C24—C25—C20 | 0.8 (5) |
N1—C1—C6—C5 | 178.3 (2) | N4—C20—C25—C24 | 174.6 (3) |
C2—C1—C6—C5 | −0.2 (4) | C21—C20—C25—C24 | −2.6 (5) |
C1—N1—C7—C8 | −173.0 (2) | C20—N4—C26—C27 | −148.9 (3) |
C10—N1—C7—C8 | 40.3 (3) | C29—N4—C26—C27 | 57.0 (3) |
C9—N2—C8—C7 | 62.2 (3) | C28—N5—C27—C26 | 56.4 (3) |
N1—C7—C8—N2 | −51.8 (3) | N4—C26—C27—N5 | −57.5 (3) |
C8—N2—C9—C10 | −61.5 (3) | C27—N5—C28—C29 | −54.8 (3) |
C1—N1—C10—C9 | 173.4 (2) | C20—N4—C29—C28 | 150.1 (2) |
C7—N1—C10—C9 | −39.5 (3) | C26—N4—C29—C28 | −55.8 (3) |
N2—C9—C10—N1 | 50.3 (3) | N5—C28—C29—N4 | 54.6 (3) |
C16—C11—C12—C13 | 0.5 (4) | C35—C30—C31—C32 | −1.0 (4) |
C17—C11—C12—C13 | −177.6 (3) | C36—C30—C31—C32 | 177.1 (3) |
C11—C12—C13—C14 | 0.4 (5) | C30—C31—C32—C33 | 1.6 (4) |
C18—O5—C14—C13 | 1.3 (5) | C37—O10—C33—C34 | 0.7 (4) |
C18—O5—C14—C15 | −178.7 (3) | C37—O10—C33—C32 | −178.7 (3) |
C12—C13—C14—O5 | 178.9 (3) | C31—C32—C33—O10 | 178.6 (3) |
C12—C13—C14—C15 | −1.0 (5) | C31—C32—C33—C34 | −0.8 (4) |
O5—C14—C15—C16 | −179.2 (3) | O10—C33—C34—C35 | −179.8 (3) |
C13—C14—C15—C16 | 0.7 (5) | C32—C33—C34—C35 | −0.5 (4) |
C14—C15—C16—C11 | 0.2 (5) | C31—C30—C35—C34 | −0.3 (4) |
C12—C11—C16—C15 | −0.8 (4) | C36—C30—C35—C34 | −178.5 (3) |
C17—C11—C16—C15 | 177.3 (3) | C33—C34—C35—C30 | 1.1 (4) |
C12—C11—C17—O4 | 2.7 (4) | C35—C30—C36—O9 | 15.2 (4) |
C16—C11—C17—O4 | −175.3 (2) | C31—C30—C36—O9 | −162.9 (3) |
C12—C11—C17—O3 | −177.3 (3) | C35—C30—C36—O8 | −166.4 (2) |
C16—C11—C17—O3 | 4.6 (4) | C31—C30—C36—O8 | 15.5 (4) |
C14—O5—C18—C19 | 178.7 (3) | C33—O10—C37—C38 | 176.2 (3) |