O1—N3 | 1.222 (3) | C8—H8B | 0.97 |
O2—N3 | 1.221 (3) | C9—C10 | 1.503 (4) |
N1—C1 | 1.376 (3) | C9—H9A | 0.97 |
N1—C10 | 1.462 (3) | C9—H9B | 0.97 |
N1—C7 | 1.469 (4) | C10—H10A | 0.97 |
N2—C8 | 1.473 (4) | C10—H10B | 0.97 |
N2—C9 | 1.479 (4) | I1—C14 | 2.090 (3) |
N2—H21 | 0.859 (18) | O3—C17 | 1.257 (3) |
N2—H22 | 0.850 (18) | O4—C17 | 1.257 (3) |
N3—C4 | 1.440 (4) | C11—C16 | 1.391 (4) |
C1—C2 | 1.400 (4) | C11—C12 | 1.395 (4) |
C1—C6 | 1.410 (4) | C11—C17 | 1.493 (4) |
C2—C3 | 1.361 (4) | C12—C13 | 1.377 (4) |
C2—H2 | 0.93 | C12—H12 | 0.93 |
C3—C4 | 1.378 (4) | C13—C14 | 1.386 (4) |
C3—H3 | 0.93 | C13—H13 | 0.93 |
C4—C5 | 1.378 (4) | C14—C15 | 1.385 (4) |
C5—C6 | 1.357 (4) | C15—C16 | 1.372 (4) |
C5—H5 | 0.93 | C15—H15 | 0.93 |
C6—H6 | 0.93 | C16—H16 | 0.93 |
C7—C8 | 1.502 (4) | O5—H1W | 0.805 (18) |
C7—H7A | 0.97 | O5—H2W | 0.805 (18) |
C7—H7B | 0.97 | O6—H4W | 0.795 (18) |
C8—H8A | 0.97 | O6—H3W | 0.800 (18) |
C1—N1—C10 | 117.2 (2) | N2—C8—H8B | 109.6 |
C1—N1—C7 | 117.8 (2) | C7—C8—H8B | 109.6 |
C10—N1—C7 | 112.8 (2) | H8A—C8—H8B | 108.1 |
C8—N2—C9 | 110.6 (2) | N2—C9—C10 | 110.3 (2) |
C8—N2—H21 | 108 (3) | N2—C9—H9A | 109.6 |
C9—N2—H21 | 115 (3) | C10—C9—H9A | 109.6 |
C8—N2—H22 | 104 (3) | N2—C9—H9B | 109.6 |
C9—N2—H22 | 118 (3) | C10—C9—H9B | 109.6 |
H21—N2—H22 | 101 (3) | H9A—C9—H9B | 108.1 |
O2—N3—O1 | 122.5 (3) | N1—C10—C9 | 111.5 (2) |
O2—N3—C4 | 119.1 (3) | N1—C10—H10A | 109.3 |
O1—N3—C4 | 118.4 (3) | C9—C10—H10A | 109.3 |
N1—C1—C2 | 121.1 (2) | N1—C10—H10B | 109.3 |
N1—C1—C6 | 121.5 (2) | C9—C10—H10B | 109.3 |
C2—C1—C6 | 117.4 (2) | H10A—C10—H10B | 108 |
C3—C2—C1 | 120.9 (3) | C16—C11—C12 | 119.5 (3) |
C3—C2—H2 | 119.6 | C16—C11—C17 | 120.4 (2) |
C1—C2—H2 | 119.6 | C12—C11—C17 | 120.1 (2) |
C2—C3—C4 | 119.9 (3) | C13—C12—C11 | 120.4 (3) |
C2—C3—H3 | 120.1 | C13—C12—H12 | 119.8 |
C4—C3—H3 | 120.1 | C11—C12—H12 | 119.8 |
C5—C4—C3 | 121.2 (3) | C12—C13—C14 | 119.0 (3) |
C5—C4—N3 | 119.5 (3) | C12—C13—H13 | 120.5 |
C3—C4—N3 | 119.3 (3) | C14—C13—H13 | 120.5 |
C6—C5—C4 | 118.9 (3) | C15—C14—C13 | 121.4 (3) |
C6—C5—H5 | 120.5 | C15—C14—I1 | 119.1 (2) |
C4—C5—H5 | 120.5 | C13—C14—I1 | 119.6 (2) |
C5—C6—C1 | 121.8 (3) | C16—C15—C14 | 119.2 (3) |
C5—C6—H6 | 119.1 | C16—C15—H15 | 120.4 |
C1—C6—H6 | 119.1 | C14—C15—H15 | 120.4 |
N1—C7—C8 | 111.9 (2) | C15—C16—C11 | 120.5 (3) |
N1—C7—H7A | 109.2 | C15—C16—H16 | 119.8 |
C8—C7—H7A | 109.2 | C11—C16—H16 | 119.8 |
N1—C7—H7B | 109.2 | O4—C17—O3 | 125.0 (3) |
C8—C7—H7B | 109.2 | O4—C17—C11 | 116.9 (2) |
H7A—C7—H7B | 107.9 | O3—C17—C11 | 118.1 (2) |
N2—C8—C7 | 110.2 (2) | H1W—O5—H2W | 101 (4) |
N2—C8—H8A | 109.6 | H4W—O6—H3W | 117 (4) |
C7—C8—H8A | 109.6 | ||
C10—N1—C1—C2 | 148.6 (3) | C9—N2—C8—C7 | 58.1 (3) |
C7—N1—C1—C2 | 8.9 (4) | N1—C7—C8—N2 | −54.7 (3) |
C10—N1—C1—C6 | −33.7 (4) | C8—N2—C9—C10 | −58.5 (3) |
C7—N1—C1—C6 | −173.4 (3) | C1—N1—C10—C9 | 165.8 (3) |
N1—C1—C2—C3 | 177.1 (3) | C7—N1—C10—C9 | −52.6 (3) |
C6—C1—C2—C3 | −0.8 (4) | N2—C9—C10—N1 | 55.3 (4) |
C1—C2—C3—C4 | 1.3 (5) | C16—C11—C12—C13 | 1.6 (4) |
C2—C3—C4—C5 | −1.0 (5) | C17—C11—C12—C13 | −179.0 (3) |
C2—C3—C4—N3 | 179.3 (3) | C11—C12—C13—C14 | −1.7 (4) |
O2—N3—C4—C5 | 6.3 (4) | C12—C13—C14—C15 | 0.1 (4) |
O1—N3—C4—C5 | −173.9 (3) | C12—C13—C14—I1 | 179.0 (2) |
O2—N3—C4—C3 | −173.9 (3) | C13—C14—C15—C16 | 1.6 (4) |
O1—N3—C4—C3 | 5.8 (4) | I1—C14—C15—C16 | −177.4 (2) |
C3—C4—C5—C6 | 0.1 (5) | C14—C15—C16—C11 | −1.6 (4) |
N3—C4—C5—C6 | 179.8 (3) | C12—C11—C16—C15 | 0.0 (4) |
C4—C5—C6—C1 | 0.4 (5) | C17—C11—C16—C15 | −179.3 (3) |
N1—C1—C6—C5 | −178.0 (3) | C16—C11—C17—O4 | −26.0 (4) |
C2—C1—C6—C5 | −0.1 (4) | C12—C11—C17—O4 | 154.6 (3) |
C1—N1—C7—C8 | −166.2 (2) | C16—C11—C17—O3 | 153.1 (3) |
C10—N1—C7—C8 | 52.5 (3) | C12—C11—C17—O3 | −26.2 (4) |