| Rigaku AFC11 with Saturn 724+ CCD diffractometer | 3129 independent reflections |
| Radiation source: Rotating Anode | 2665 reflections with I > 2σ(I) |
| Detector resolution: 28.5714 pixels mm-1 | Rint = 0.024 |
| ω scans | θmax = 27.5°, θmin = 3.1° |
| Absorption correction: multi-scan (REQAB; Rigaku, 1998) | h = −10→10 |
| Tmin = 0.904, Tmax = 1.000 | k = −12→11 |
| 11199 measured reflections | l = −23→22 |