| Rigaku AFC11 with Saturn 724+ CCD diffractometer | 4392 independent reflections |
| Radiation source: Rotating Anode | 3240 reflections with I > 2σ(I) |
| Detector resolution: 28.5714 pixels mm-1 | Rint = 0.041 |
| ω scans | θmax = 27.5°, θmin = 3.3° |
| Absorption correction: multi-scan (REQAB; Rigaku, 1998) | h = −10→11 |
| Tmin = 0.828, Tmax = 1.000 | k = −13→13 |
| 8155 measured reflections | l = −14→11 |