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. 2022 Apr 28;78(Pt 5):530–535. doi: 10.1107/S2056989022004388
Bruker AXS D8 QUEST, Photon III detector diffractometer 4177 independent reflections
Radiation source: fine-focus sealed X-Ray tube 3809 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.102
Detector resolution: 7.31 pixels mm-1 θmax = 30.0°, θmin = 2.6°
φ and ω shutterless scans h = −22→22
Absorption correction: multi-scan (SADABS; Krause et al., 2015) k = −9→9
Tmin = 0.415, Tmax = 0.747 l = −17→17
44165 measured reflections