Bruker AXS D8 QUEST, Photon III detector diffractometer | 4177 independent reflections |
Radiation source: fine-focus sealed X-Ray tube | 3809 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.102 |
Detector resolution: 7.31 pixels mm-1 | θmax = 30.0°, θmin = 2.6° |
φ and ω shutterless scans | h = −22→22 |
Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −9→9 |
Tmin = 0.415, Tmax = 0.747 | l = −17→17 |
44165 measured reflections |