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. 2022 Apr 28;78(Pt 5):536–539. doi: 10.1107/S2056989022004339

Table 3. Experimental details.

Crystal data
Chemical formula [Eu(C8H4O4)(CH3O2)(H2O)]
M r 393.13
Crystal system, space group Monoclinic, C2/c
Temperature (K) 293
a, b, c (Å) 26.5184 (15), 7.2632 (2), 15.3622 (8)
β (°) 130.906 (9)
V3) 2236.3 (3)
Z 8
Radiation type Mo Kα
μ (mm−1) 5.63
Crystal size (mm) 0.2 × 0.1 × 0.1
 
Data collection
Diffractometer Rigaku SuperNova, single source at offset/far, HyPix3000
Absorption correction Multi-scan (CrysAlis PRO; Rigaku OD, 2019)
T min, T max 0.218, 1.000
No. of measured, independent and observed [I > 2σ(I)] reflections 9923, 2393, 2138
R int 0.032
(sin θ/λ)max−1) 0.648
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.024, 0.052, 1.05
No. of reflections 2393
No. of parameters 167
No. of restraints 1
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.64, −0.79

Computer programs: CrysAlis PRO (Rigaku OD, 2019), SHELXT2018/2 (Sheldrick, 2015a ), SHELXL2018/3 (Sheldrick, 2015b ) and OLEX2 (Dolomanov et al., 2009).