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. 2019 Oct 22;9(58):33957–33968. doi: 10.1039/c9ra07988b

1H and 13C NMR data of 10–11 in CD3ODa.

Position 10 11
δ H δ C δ H δ C
1 4.25 q (6.5) 80.8 3.96 t (6.5) 85.7
2 1.38 d (6.5) 23.8 1.61 m, 1.78 m 30.4
3 0.85 t (7.5) 9.2
1′ 134.9 132.5
2′ 6.59 s 104.2 6.55 s 103.5
3′ 149.4 147.8
4′ 135.8 134.6
5′ 149.4 147.8
6′ 6.59 s 104.2 6.55 s 103.5
graphic file with name c9ra07988b-t3.jpg 3.19 s 56.1 3.18 s 55.2
graphic file with name c9ra07988b-t4.jpg 3.84 s 56.3 3.83 s 55.3
graphic file with name c9ra07988b-t5.jpg 3.84 s 56.3 3.83 s 55.3
a

Signal multiplicity and coupling constants (Hz) are in parentheses. The assignments were based on HSQC, HMBC, and 1H–1H COSY experiments; NMR data were measured using NMR spectrometers operating at 850 MHz for 10 and 800 MHz for 11.