Skip to main content
. 2018 Feb 14;8(13):7243–7251. doi: 10.1039/c7ra11896a

The determination and recovery of Co(ii) in vitamin B12 samples by the proposed method and FAAS (n = 3).

Sample Spiked (mg g−1) VALS-DLLME FAAS
Found (mg g−1) Recovery (%) RSD (%) Found (mg g−1) Recovery (%) RSD (%)
No. I (1 tablet = 0.1509 g) 0.000 0.729 0.762
0.165 0.868 94.1 1.24 0.888 94.0 2.49
0.331 1.054 99.6 2.43 1.067 101.8 1.57
0.994 1.736 101.1 1.09 1.749 102.3 0.98
No. II (1 tablet = 0.1374 g) 0.000 0.699 0.706
0.182 0.859 86.0 1.54 0.888 99.0 1.26
0.364 1.077 102.7 0.98 1.084 103.0 2.37
1.092 1.776 99.7 2.32 1.849 104.3 1.57
No. III (1 tablet = 0.1270 g) 0.000 0.701 0.702
0.197 0.882 92.0 1.43 0.898 98.0 1.43
0.394 1.087 99.5 1.57 1.118 104.5 1.89
1.181 1.882 100.7 0.69 1.953 105.7 0.94
No. IV (1 tablet = 0.3056 g) 0.000 0.111 0.115
0.081 0.187 92.0 2.12 0.193 93.1 2.31
0.164 0.272 97.0 3.45 0.275 99.0 1.54
0.491 0.605 100.7 1.34 0.612 101.0 0.92
No. V (1 tablet = 0.3924 g) 0.000 0.036 0.038
0.064 0.097 96.0 1.57 0.092 84.0 1.27
0.127 0.163 98.5 2.58 0.168 102.4 0.93
0.382 0.415 99.3 2.63 0.426 101.3 1.38