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. 2018 Feb 26;8(16):8761–8769. doi: 10.1039/c8ra00485d

Influence of different catalysts for synthesis of pentafulvenea.

Entry Catalyst Yieldb (%)
1 KCC-1
2 Fe3O4/KCC-1/APTPOSS
3 Fe3O4/KCC-1/APTPOSS/salen/Pd(ii) 92
4 Nano-SiO2/salen/Pd(ii) 53
5 MCM-41/salen/Pd(ii) 74
6 SBA-15/salen/Pd(ii) 80
7 Salen/Pd(ii) 83
a

Reaction conditions: 2-acetyl-benzaldehyde (10 mmol), cyclopentadiene (70 mmol), and catalyst (6 mg), at room temperature for 3 h.

b

Isolated yield.