Reaction of various 2-acetyl-benzaldehydes with cyclopentadiene in the presence of Fe3O4/KCC-1/APTPOSS/salen/Pd(ii) MNPsa.
Entry | 2-Acetyl-benzaldehyde | Product | Yieldb (%) |
---|---|---|---|
1 | 92 | ||
2 | 94 | ||
3 | 89 | ||
4 | 87 | ||
5 | 90 | ||
6 | 91 |
Reaction conditions: 2-acetyl-benzaldehyde (10 mmol), cyclopentadiene (70 mmol), and catalyst (6 mg), at room temperature for 3 h.
Isolated yields (%).