Onset temperatures of 3a–ca.
| Compd. | Onset temp. Ar [°C] | Onset temp. O2 [°C] |
|---|---|---|
| 3a | 152 | 166 |
| 3b | 253 | 243 |
| 3c | 120 | 233 |
Ar, O2 (gas flow 20 mL min−1) (Ar carrier gas flow 40 mL min−1, heating rate 10 °C min−1).
| Compd. | Onset temp. Ar [°C] | Onset temp. O2 [°C] |
|---|---|---|
| 3a | 152 | 166 |
| 3b | 253 | 243 |
| 3c | 120 | 233 |
Ar, O2 (gas flow 20 mL min−1) (Ar carrier gas flow 40 mL min−1, heating rate 10 °C min−1).