The crystal data and structure parameters of compounds A and C.
| Compound A13 | Compound C | |
|---|---|---|
| Empirical formula | Zn6C27H32O31 | NaZnC9H14O11.5 |
| Formula weight | 1244.75 | 394.56 |
| Temperature (K) | 298 | 296(2) |
| Wavelength | 0.71073 | 0.71073 |
| Crystal system | Trigonal | Triclinic |
| Space group | R3c | P1̄ |
| a (Å) | 30.159(4) | 7.0980(11) |
| b (Å) | 30.159(4) | 9.8000(16) |
| c (Å) | 6.9280(14) | 11.2043(17) |
| α (deg) | 90 | 66.923 |
| β (deg) | 90 | 73.598 |
| γ (deg) | 120 | 84.720 |
| Volume (Å3) | 5457.2(16) | 687.68(19) |
| Z | 6 | 2 |
| Density (g cm−3) | 2.273 | 1.88 |
| F (0 0 0) | 3732 | 402 |
| Crystal size (mm3) | 0.15 × 0.15 × 0.30 | 0.05 × 0.03 × 0.02 |
| Theta range for data collection (deg) | 2.34, 33.49 | 2.30, 32.0 |
| Absorption correction | Multi-scan | Multi-scan |
| Goodness-of-fit on F2 | 1.004 | 0.97 |
| Final R indices [I > 2sigma(I)] | 0.0519, 0.1281 | 0.0510, 0.1329 |
| R indices (all data) | 0.0619, 0.1348 | 0.0977, 0.1130 |
| Largest diff. peak and hole (Å−3) | 2.42, −0.79 | 0.79, −0.69 |