Optimization at the CO2 pressure of 3.0 MPaa.
| Entry | Catalyst concentration (mol%) | Time (h) | Yield (%) |
|---|---|---|---|
| 1 | 8 | 30 | 99 |
| 2 | 4 | 30 | 99 |
| 3 | 2 | 30 | 93 |
| 4 | 4 | 20 | 99 |
| 5 | 4 | 10 | 85 |
| 6 | 3 | 20 | 93 |
a
Reaction conditions: reaction temperature: 120 °C, CO2 pressure: 3.0 MPa.
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