13C NMR data of 1–6 in DMSO-d6a.
1 | 2 | 3 | 4 | 5 | 6 | |
---|---|---|---|---|---|---|
1 | 170.4 | 170.0, C | 168.6, C | 169.0, C | 170.2, C | |
2 | 101.9, C | |||||
3 | 65.4, CH | 64.4, CH | 84.2, C | 48.6, CH | 163.2, C | 51.7, C |
4 | 150.2, C | 149.9, C | 151.5, C | 153.3, C | 148.9, C | 126.7, C |
5 | 124.2, CH | |||||
6 | 147.5, C | 147.2, C | 146.6, C | 146.6, C | 145.7, C | 121.6, CH |
7 | 127.2, CH | 127.2, CH | 127.9, CH | 127.0, CH | 127.7, CH | 127.5, CH |
8 | 134.6, CH | 134.6, CH | 134.7, CH | 134.5, CH | 135.6, CH | 110.7, CH |
9 | 126.8, CH | 126.8, CH | 127.5, CH | 126.8, CH | 128.7, CH | 148.3, C |
10 | 126.1, CH | 126.2, CH | 126.4, CH | 126.5, CH | 126.5, CH | 101.9, CH |
11 | 120.0, C | 120.2, C | 120.7, C | 120.1, C | 121.1, C | 142.7, C |
12 | 159.8, C | 159.9, C | 158.9, C | 160.3, C | 160.1, C | 159.4, C |
13 | 52.8, CH | |||||
14 | 53.7, CH | 53.3, CH | 52.8, CH | 51.8, CH | 54.9, CH | 173.7, C |
15 | 34.7, CH2 | 33.7, CH2 | 33.7, CH2 | 35.5, CH2 | 30.9, CH2 | 14.1, CH3 |
16 | 74.8, C | 77.4, C | 86.4, C | 80.1, C | 86.3, C | 42.1, C |
17 | 78.4, CH | 82.0, CH | 88.5, CH | 88.2, CH | 83.5, CH | 144.5, CH |
18 | 112.7, CH2 | |||||
19 | 136.0, C | 139.0, C | 136.6, C | 137.3, C | 142.0, C | 24.4, CH3 |
20 | 113.9, CH | 116.6, CH | 114.4, CH | 115.1, CH | 117.5, CH | 23.6, CH3 |
21 | 129.6, CH | 129.4, CH | 129.8, CH | 128.9, CH | 131.6, CH | |
22 | 124.6, CH | 125.4, CH | 125.2, CH | 124.7, CH | 126.0, CH | |
23 | 124.7, CH | 123.9, CH | 126.3, CH | 125.5, CH | 125.3, CH | |
24 | 139.0, C | 137.9, C | 137.4, C | 138.7, C | 131.6, C | |
25 | 62.5, CH | 67.6, CH | 68.0, CH | 68.3, CH | 45.9, C | |
26 | 165.7, C | 170.2, C | 171.6, C | 172.3, C | 177.8, C | |
27 | 14.8, CH3 | 59.2, CH2 | 38.1, CH | 37.8, CH | 17.0, CH2 | |
28 | 15.0, CH3 | 15.1, CH3 | 11.8, CH2 | |||
29 | 24.5, CH2 | 24.50, CH2 | ||||
30 | 11.3, CH3 | 11.6, CH3 | ||||
31 | 23.8, CH3 | 16.6, CH3 |
Recorded at 100 MHz.