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. 2022 Apr 20;7(17):14666–14677. doi: 10.1021/acsomega.1c07230

Table 2. Experimental Ranges of the Independent Variables.

    coded level
process independent variable –1.682 –1 0 +1 +1.682
first step M1: methanol (vol %) 19.8 30.0 45.0 60.0 70.2
S1: sulfuric acid (vol %) 0.8 2.5 5 7.5 9.2
L1: length of ultrasound clamp (mm) 100 200 400 600 700
second step M2: methanol (vol %) 26.4 40 60 80 93.6
S2: sulfuric acid (vol %) 0.6 2 4 6 7.4
L2: length of ultrasound clamp (mm) 100 200 400 600 700