Fig. 1. Solid-state structure of [Ni30S16(PEt3)11]·Et2O (1·Et2O) from two different orientations. (A and B) Ni21 core. (C and D) The three [cyclo-{Ni(μ-S)}3] units attached to the Ni21S7 core. (E and F) Ni-only structure of 1. (G and H) Full molecular structure. Color scheme: Nishell, green; Nicore, blue; S, yellow; P, orange; C, grey. Carbon atoms are shown in wireframe. Diethyl ether solvate molecule and hydrogen atoms were omitted for clarity.
